Firing Effects

The glaze longquan_iron_mashiko_0 with three different firing protocols.

The first firing drops from top temperature to 1750 deg F at 300 deg F an hour. This rate of temperature
drop is an approximation to "dropping like a stone", yet slow enough that the multiple zones in the kiln can
maintain nearly the same temperature.

The second firing drops only to 2210 deg F at that rapid rate of 300 deg F an hour. It then has a one-hour hold,
then drops to 1900 deg F at only 80 deg F an hour.

The third firing has a Two-hour hold on the way up, before maturation, at 2250 deg F, 60 degrees below the
top temperature.

The primary difference between these three firings is that slowing down of the firing at a temperature
near the top, but not so high that a higher cone would thereby be reached.

The first firing has no hold, in the second firing, the hold is on the way down, and in the third,
on the way up.

I have previously noticed that glazes high in mica seem more "melted" with a hold near maturation.
This is an exploration of the effect of such holds on a oil spot glaze, seen here:



Image of the glaze longquan_iron_mashiko_0 in Firing 1

full view

inside



full view

outside

bowl is ~ 4 inches in diameter.



Image of the glaze longquan_iron_mashiko_0 in Firing 2

full view

inside



full view

outside

bowl is ~ 4 inches in diameter.



Image of the glaze longquan_iron_mashiko_0 in Firing 3

full view

inside



full view

outside

bowl is ~ 4 inches in diameter.



oxidation firing to cone 10 in an electric kiln

The third firing is a hot cone 10, perhaps cone 10 and a half.

Firing profile 1

Up Fire profile

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2050 deg F

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile

300 deg F an hour to 1750 deg F then a half hour hold at 1750 deg F

300 deg F an hour to 1700 deg F then a Three hour hold at 1700 deg F

25 deg F an hour to 1650 deg F then a one hour hold at 1650 deg F



Firing profile 2

Up Fire profile

150 deg F an hour to 250 deg F

400 deg F an hour to 2050 deg F then a hold of 20 min

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile

300 deg F an hour to 2210 deg F then a one hour hold at 2210 deg F

80 deg F an hour to 1900 deg F

300 deg F an hour to 1750 deg F then a half hour hold at 1750 deg F

300 deg F an hour to 1700 deg F then a Two hour hold at 1700 deg F

300 deg F an hour to 1600 deg F then a Two hour hold at 1600 deg F



Firing profile 3

Up Fire profile

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2050 deg F

120 deg F an hour to 2250 deg F then a two hour hold at 2250 deg F.

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile

300 deg F an hour to 1750 deg F then a half hour hold at 1750 deg F

300 deg F an hour to 1700 deg F then a Three hour hold at 1700 deg F

25 deg F an hour to 1650 deg F then a one hour hold at 1650 deg F



Clay body is a grolleg porcelain from Tacoma Clay Art Center.



glaze compositions

Empirical Formula longquan_iron_mashiko_0 :

K2O        0.11
Na2O       0.45
Li2O       0.15
CaO        0.11
MgO        0.18

Al2O3      0.71
Fe2O3      0.19

SiO2       4.27

molecular percent Silica 69%



Remarks

In the first firing, where thickly applied, this glaze is a full gloss, inky black with silvery-bronze markings.
Where thinly applied the entire field is covered in what appears to be etched metallic bronze markings.

In the second firing, a thicker application of glaze is required to allow the glossy black matrix visibility.
The outside of the bowl, with a similar quantity of glaze as the pot seen in the first firing is now entirely covered in the
metallic bronze crystals.

In the third firing, with an even thicker glaze application, the bronze colored crystals almost entirely
cover both inside and outside of the bowl. The pinholes are the result of the thickness of the glaze application.

The hold before peak temperature in the last firing, is considerably hotter than the hold after peak temperature
in the second firing. It is therefore unclear if the increased effect seen in the third firing is a result of the
higher temperature, or the positioning of the hold before rather than after peak temperature.

More time at a higher temperature allows more crystal growth. The cones in all three firings are nearly the same.

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