The effect of distinct Firings on a Glaze

The glaze satIron_ZG_1S_Z3J seen in two distinct firing protocols.

Both firings are to Cone 10 in an electric Kiln, though the first firing is a hot cone 10,
with the cone 11 slightly more than tipped.

The first firing is slowed on the way up with an hour hold at 2170 deg F, and an additional half-hour hold at
2270 deg F. In addition, it has a slower temperature rise for the last segments of the up part of the firing.

The intent had been to increase the time available for slower reacting materials to enter the glaze melt,
without firing to a higher cone. This result was only partially achieved.

The second firing was comprised of a much faster ramp up, but holds on the way down at 1750 deg F, 1700 deg F,
and 1650 deg F. In the second firing, the glaze is orangy-brown, with a dusting of metallic coppery colored particles.
In the bottom where the glaze is a bit thicker is seen a thin broken black outline of a hexagonal
cellular structure.

It is interesting that the result of increasing the total firing time and adding holds near the top temperature
seems to have been to create an oil spot glaze in the first firing. One is tempted to imagine that the faint
outline of a cellular structure visible in the bottom of the bowl fired fast, in the second firing, grew
into the dominant black matrix of the oil spot glaze, while the interiors of the cells shrunk to the visible
oil spots seen in the first firing.

The holds on the way down in the first firing differ as well, an artifact of the inconvenience of programming
more than 8 ramps for the kiln controller. I doubt that the difference in holds at a low
temperature are relevant to the formation of an oil spot glaze.

The inlay design in the bowl in the second firing is glazed with inlay_Z3K.

The design is created by adhering a mask and then applying the main glaze. After drying,
the mask is removed and the open area filled in with a second glaze, using a bulb syringe
with a needle applicator.



Image of the glaze satIron_ZG_1S_Z3J in Firing One

full view

inside

full view

outside

bowl is ~ 4 inches in diameter.



Image of the glaze satIron_ZG_1S_Z3J in Firing Two

full view

Inlay glaze is inlay_Z3K_0

bowl is ~5 inches in diameter.



oxidation firing to cone 10 in an electric kiln

Firing profiles

First Firing

Up Fire profile Firing 1

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2170 deg F with a hold of 1 hour at 2170 deg F

120 deg F an hour to 2250 deg F

60 deg F an hour to 2270 deg F with a hold of 30 minutes at 2270 deg F

60 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile Firing 1

300 deg F an hour to 1750 deg F then a 4 hour hold at 1750 deg F

25 deg F an hour to 1650 deg F then a one hour hold at 1650 deg F



Second Firing

Up Fire profile Firing 2

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2050 deg F

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile Firing 2

300 deg F an hour to 1800 deg F then a 2 hr hold at 1800 deg F

300 deg F an hour to 1750 deg F then a 1 hr hold at 1750 deg F

50 deg F an hour to 1700 deg F then a three hour hold at 1700 deg F

25 deg F an hour to 1650 deg F then a one hour hold at 1650 deg F

Clay body is a grolleg porcelain from Tacoma Clay Art Center.



glaze composition

Empirical Formula satIron_ZG_1S_Z3J:

K2O        0.33
Na2O       0.48
CaO        0.18
MgO        0.01

Al2O3      0.50
Fe2O3      0.17

SiO2       3.4
P2O5       0.17

molecular percent Silica 64.7%



Empirical Formula inlay_Z3K_0 :

K2O        0.14
Na2O       0.82
CaO        0.02
MgO        0.02

Al2O3      0.58
Fe2O3      0.02

SiO2       2.31
P2O5       0.18

molecular percent Silica 56.5%



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