iron colors in firings with several holds

The glaze, wisskirchen-crystals-PAl in simplified firings is
shown here .

Those firings has holds only at the temperatures 1650 degF and 1900 degF. Here we elaborate on
those firings by including both of those holds in various orders in each of these firings.

This is a continued exploration of the effect of holds in the down-fire of a saturated iron glaze. All of
the down-fire holds in these firings are at either 1650 deg F, or at 1900 deg F. These firings however
will have a hold at both of these temperatures.

I wish to see the effects of two down-fire holds, and in particular explore the effect of
interchanging the order of the holds.

I fired this glaze, wisskirchen-crystals-PAl in four distinct firings. All four firings have the same
up-fire protocol.

Firing 1:

In the down-fire, there is one four hour hold at 1900 degF, followed by a four hour hold at 1650 degF.

Firing 2:

In the down-fire, there is one four hour hold at 1650 degF, followed by a four hour hold at 1900 degF.

Firing 3:

In the down-fire, there is one four hour hold at 1650 degF, followed by a four hour hold at 1900 degF,
followed by a four hour hold at 1650 degF.

Firing 4:

In the down-fire, there is one eight hour hold at 1650 degF followed by a four hour hold at 1900 degF.

The down-fire of Firing 2 reverses the order of the holds of the down-fire of firing 1. Likewise the
Firing 7 has all of the hold time at 1650 degF preceding the hold at 1900 degF.

Firings 1 and 2 are a pair of firings which differ only in the order of the down-fire holds. Likewise
Firing 6 and Firing 7. I ask if the order of the holds is relevant or only the time in the holds?
The answer for this glaze seems to be yes.



Image of the glaze wisskirchen-crystals-PAl in Firing 1

full view

full view



Image of the glaze wisskirchen-crystals-PAl in Firing 2

full view

full view



Image of the glaze wisskirchen-crystals-PAl in Firing 3

full view

full view



Image of the glaze wisskirchen-crystals-PAl in Firing 4

full view

full view



The bowls are ~4 inches in diameter.



oxidation firing to cone 10 in an electric kiln

Firing profiles

Firing 1 profile

Up Fire profile cone 10

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2050 deg F

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile cone 10

300 deg F an hour to 1900 deg F then a 4 hour hold at 1900 deg F

300 deg F an hour to 1650 deg F then a 4 hour hold at 1650 deg F



Firing 2 profile

Up Fire profile cone 10

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2050 deg F

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile cone 10

300 deg F an hour to 1650 deg F then a 4 hour hold at 1650 deg F

400 deg F an hour to 1900 deg F then a 4 hour hold at 1900 deg F



Firing 3 profile

Up Fire profile cone 10

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2050 deg F

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile cone 10

300 deg F an hour to 1650 deg F then a 4 hour hold at 1650 deg F

400 deg F an hour to 1900 deg F then a 4 hour hold at 1900 deg F

300 deg F an hour to 1650 deg F then a 4 hour hold at 1650 deg F



Firing 4 profile

Up Fire profile cone 10

150 deg F an hour to 250 deg F

400 deg F an hour to 1800 deg F

300 deg F an hour to 2050 deg F

120 deg F an hour to 2310 deg F with a hold of 20 minutes at 2310 deg F

Down Fire Profile cone 10

300 deg F an hour to 1650 deg F then an 8 hour hold at 1650 deg F

400 deg F an hour to 1900 deg F then a 4 hour hold at 1900 deg F



Clay body is a grolleg porcelain from Clay Art Center in Tacoma, WA.



glaze composition

Empirical Formula wisskirchen-crystals-PAl:

K2O        0.10
Na2O       0.24
CaO        0.62
MgO        0.04

Al2O3      0.55
Fe2O3      0.31

SiO2       3.45
TiO2       0.03

molecular percent Silica 64.6%



Remarks

These are some of the additional firings with distinct down-fire protocols, and distinct results,
to which I aluded in my prior note.

Comparing wisskirchen-crystals-PAl in firing 2 to firing 1:

There is a greater degree of intermixing of dark and light colored markings, and a greater preponderance of
dark markings. In the inside of the firing 2 bowl there are matte yellow clusters in a dark glassy matrix,
which are not seen in firing 1.

comparing wisskirchen-crystals-PAl in firing 4 to firing 3:

Markings resembling dendritic growths are seen on the outside of the firing 4 bowl, and the surface
of the outside has a waxy near gloss, all in contrast to that seen in Firing 3. Additionally, the matte yellow
clusters in the dark glassy matrix as seen in Firing 2 are seen here.

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